Part I Principles- 1. Introduction- 2. Solid state NMR approach 2.1. CP-MAS and DD-MAS NMR 2.2. Quadrupolar nuclei - 3. Brief outline of NMR parameters 3.1. Chemical shifts 3.2. Relaxation parameters 3.3. Dynamics-dependent suppression of peaks- 4. Multinuclear approaches 4.1. 31P NMR 4.2. 2H NMR 4.3. 17O NMR- 5. Experimental strategies 5.1. Isotope enrichment (labeling) 5.2. Assignment of peaks 5.3. Ultra high-field and ultra high-speed MAS NMR spectroscopy- 6. NMR constraints for structural determination 6.1. Orientational constraint 6.2. Interatomic distance 6.3. Torsion angles 6.4. Conformation-dependent 13C chemical shifts - 7. Dynamics 7.1. Fast motions with motional frequency 106 Hz 7.2. Intermediate or slow motions with frequency between 106 and 103 Hz 7.3. Very slow motions with frequency
EAN/ISBN : 9781402043031
Publisher(s): Springer Netherlands
Discussed keywords: Biopolymere, Festkörper, Kernresonanzspektroskopie
Format: ePub/PDF

Author(s): Saito, Hazime - Ando, Isao - Naito, Akira